Buchi NIRMaste Pro IP65 Bedienungsanleitung

Operation Manual11593580 enNIRMaster ®

2 Safety10 NIRMaster Operation Manual, Version B2.5.2 Warning labels on housing and assembliesThe following warning sticker(s) can be found on the ho

2 Safety11 NIRMaster Operation Manual, Version B2.5.4 Built-in safety elements and measuresThe instrument is equipped with the following safety eleme

3 Technical data12 NIRMaster Operation Manual, Version B3 Technical dataThis section introduces the reader to the instrument specifications. It conta

3 Technical data13 NIRMaster Operation Manual, Version BTechnical data NIRMaster Dimensions and weightIP 54 IP 54 Pro IP 65 ProHeight 360 mm 360 mm 3

3 Technical data14 NIRMaster Operation Manual, Version B3.1 Materials usedMaterials usedComponent Material designationSpectrometer base AluminumWedg

4 Description of function15 NIRMaster Operation Manual, Version B4 Description of functionThis section explains the basic principle of the instrumen

4 Description of function16 NIRMaster Operation Manual, Version BReference laser controlThe laser deliveres a constant, wavelength-stable beam of 633

4 Description of function17 NIRMaster Operation Manual, Version BData processing and interferogram analysisThe NIR light interacts with the sample G

4 Description of function18 NIRMaster Operation Manual, Version BFactors that can influence the measurement:• Not enough sample material available•

4 Description of function19 NIRMaster Operation Manual, Version B4.3 NIRWare software suiteNIRWare is the interface program suite between the instru

5 Putting into operation20 NIRMaster Operation Manual, Version B5 Putting into operationThis section lists the basic environmental installation requ

5 Putting into operation21 NIRMaster Operation Manual, Version B NOTICERisk of instrument damage by liquid and particle ingress• Store and operate t

5 Putting into operation22 NIRMaster Operation Manual, Version BBasic installation conditions! DANGERDeath or serious injuries by use in explosive en

5 Putting into operation23 NIRMaster Operation Manual, Version BNOTE• To cut the power in case of an emergency by unplugging, the instrument or any

6 Operation24 NIRMaster Operation Manual, Version B6 OperationThis section describes how to start a measurement and how to prepare a reference measure

6 Operation25 NIRMaster Operation Manual, Version BPreconfigured Windows login accountsUser name Minimum skill level Intended use of this accountAdmini

6 Operation26 NIRMaster Operation Manual, Version B6.2.1 Temperature tests in detailThe system is equipped with numerous temperature sensors. Individ

6 Operation27 NIRMaster Operation Manual, Version B6.3.1 Performing a reference measurementAfter the expiration of a predefined time interval (60 min.

6 Operation28 NIRMaster Operation Manual, Version BExternal reference positioning for XL addon (without Spinner):NOTEFor proper device calibration, th

6 Operation29 NIRMaster Operation Manual, Version BTransflectance adapter positioning with / without Spinner:NOTEFor proper device calibration, the Tra

Table of contents3 NIRMaster Operation Manual, Version BTable of contents1 About this manual . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 Operation30 NIRMaster Operation Manual, Version B6.3.2 Frequency of reference measurementAn additional External reference measurement is mandatory:

6 Operation31 NIRMaster Operation Manual, Version B6.4.1 Starting the NIRMaster Operator softwareThe Operator software can be set to start automatica

6 Operation32 NIRMaster Operation Manual, Version B6.4.2 Button overviewButtons ‘Wizard’Button Functionality‘Wizard’‘Go back’‘Next’‘Exit’‘Checkmark’

6 Operation33 NIRMaster Operation Manual, Version B6.4.3 Program loginAfter every program start, the user must login (see example below) with a valid

6 Operation34 NIRMaster Operation Manual, Version B6.5.1 Step 1 — Select an applicationAfter login, Press the ‘Wizard’ button to start the software w

6 Operation35 NIRMaster Operation Manual, Version B6.5.2 Step 2 — Select / create a batch for the sampleThe batch manager is a convenient tool to han

6 Operation36 NIRMaster Operation Manual, Version BPress the ‘Next’ button to proceed with the batch manager or close the wizard with the ‘Exit’ butto

6 Operation37 NIRMaster Operation Manual, Version B6.5.3 Step 3 — Perform a measurementBy standard, a reference measurement is requested prior to the

6 Operation38 NIRMaster Operation Manual, Version B‘Overview’ tab• Standard tab view• Shows the main measurement value as defined in the applicationN

6 Operation39 NIRMaster Operation Manual, Version B‘Results’ tab• View and print a detailed report.• Offers comprehensive toolbar for report handli

Table of contents4 NIRMaster Operation Manual, Version B6.5.6 Start new / rerun / close measurement . . . . . . . . . . . . . . . . . . . . . . . .

6 Operation40 NIRMaster Operation Manual, Version B‘Spectra’ • View detailed spectrum-graph• Print graph by pressing the printer button

6 Operation41 NIRMaster Operation Manual, Version B6.5.5 No / invalid resultIf a result is invalid, it will be displayed with a red background to ma

6 Operation42 NIRMaster Operation Manual, Version B6.6 Shutting down the NIRMaster 6.6.1 Standard shutdown instructionsPress the on/off button on th

7 Maintenance and repairs43 NIRMaster Operation Manual, Version B7 Maintenance and repairsThis section gives instructions on all maintenance work to

7 Maintenance and repairs44 NIRMaster Operation Manual, Version B7.2.1 HousingClean the housing with a soft, lint free damp cloth with mild soapy wat

7 Maintenance and repairs45 NIRMaster Operation Manual, Version B7.2.2 External referenceFor dependable reference measurements the External referenc

7 Maintenance and repairs46 NIRMaster Operation Manual, Version B7.2.4 Add-ons and custom sample vesselsMany sample vessels made of glass only, such

7 Maintenance and repairs47 NIRMaster Operation Manual, Version B7.3.2 Backup on USB storage devicesA simple variant for backups is to connect an ex

7 Maintenance and repairs48 NIRMaster Operation Manual, Version BPX0852abCover bodySleeve nutNOTEWith the flash drive cover installed, the NIRMaster i

7 Maintenance and repairs49 NIRMaster Operation Manual, Version BNetworkNOTEFor information about network settings and available network drive(s) con

1 About this manual5 NIRMaster Operation Manual, Version B1 About this manualThis manual describes the NIRMaster including its standard software and

7 Maintenance and repairs50 NIRMaster Operation Manual, Version BLockedUnlocked NOTICERisk of instrument damage by ingress of particles.• Check prop

7 Maintenance and repairs51 NIRMaster Operation Manual, Version BCooling airflowNOTEWhen changing the outer filters, do not tilt the NIRMaster – direct

7 Maintenance and repairs52 NIRMaster Operation Manual, Version BInner filtersThe inner filters are the second filter stage.• Lift off the top cover to

7 Maintenance and repairs53 NIRMaster Operation Manual, Version B7.6 NIRMaster basic instrumentThe drawing below shows the main components of the NI

7 Maintenance and repairs54 NIRMaster Operation Manual, Version B7.6.2 Lamp exchangeThe light source of the NIRMaster has a life expectancy of appro

8 Troubleshooting55 NIRMaster Operation Manual, Version BHow to replace the primary lamp module• Switch OFF the instrument.• Lift off the top cover

8 Troubleshooting56 NIRMaster Operation Manual, Version B7.7 Laser unitOver its lifetime, the intensity of the laser light will decrease. Thus, it is

8 Troubleshooting57 NIRMaster Operation Manual, Version B8 TroubleshootingThis section helps to resume operation after a problem has occurred with the

8 Troubleshooting58 NIRMaster Operation Manual, Version BStartExitAfter diagnostic check, basic information about the software version, timestamp and

8 Troubleshooting59 NIRMaster Operation Manual, Version B8.3 Reference measurement failsWhen the deviation between the stored reference spectrum is o

2 Safety6 NIRMaster Operation Manual, Version B2 SafetyThis section introduces the safety concept of the instrument and contains general rules of beha

8 Troubleshooting60 NIRMaster Operation Manual, Version BButtons ‘External Reference Deviation’Button Functionality‘Exit’‘Rerun’‘Checkmark’NOTEAfter l

9 Storage, transport and disposal61 NIRMaster Operation Manual, Version B9 Storage, transport and disposalThis section instructs how to handle the i

9 Storage, transport and disposal62 NIRMaster Operation Manual, Version B9.2 Transportation lockThe NIRMaster is equipped with a mechanical transpor

9 Storage, transport and disposal63 NIRMaster Operation Manual, Version BLockedLockedUnlockAfter turning the transportation lock the housing has to b

10 Spare parts64 NIRMaster Operation Manual, Version B10 Spare parts and accessoriesThis section lists spare parts, accessories and options of the

10 Spare parts65 NIRMaster Operation Manual, Version B10.2 Spare parts, optional accessories and consumablesExampleSpare partsDescription Order no.M

10 Spare parts66 NIRMaster Operation Manual, Version BSpare partsDescription Order no.External reference 11056371Spinner (Easy-Spin drive) 11056771Sp

10 Spare parts67 NIRMaster Operation Manual, Version BSpare partsDescription Order no.Set of 10 glass petri dishes (inner diameter 100 mm) for NIRFl

11 Declarations and requirements68 NIRMaster Operation Manual, Version B11 Declarations and requirements11.1 FCC requirements (for USA and Canada)E

11 Declarations and requirements69 NIRMaster Operation Manual, Version B11.2 Declaration of conformity

2 Safety7 NIRMaster Operation Manual, Version B2.4 Safety warnings and safety signs used in this manualDANGER, WARNING, CAUTION and NOTICE are standa

11 Declarations and requirements70 NIRMaster Operation Manual, Version B Health and Safety Clearance Health and Safety Clearance_20081110.doc_200811

BÜCHI Labortechnik AGCH-9230 Flawil 1 / SwitzerlandT +41 71 394 63 63 F +41 71 394 65 65 www.buchi.com Quality in your hands

2 Safety8 NIRMaster Operation Manual, Version BSymbol MeaningExplosive gases, explosive environmentHot item, hot surfaceDevice damageInhalation of sub

2 Safety9 NIRMaster Operation Manual, Version BAdditional user informationParagraphs starting with NOTE contain helpful information for working with t