Buchi Melting Point M-565 Bedienungsanleitung

Operation ManualMelting PointM�565093256 en

3 Technical data10 Melting Point M-565 Operation Manual, Version DTable 3-1: Standard accessories (cont.)Product Order numberSample holder 11055014Cl

3 Technical data11 Melting Point M-565 Operation Manual, Version D3.1.2 Optional accessoriesTable 3-2: Optional accessoriesProduct Order numberMelti

3 Technical data12 Melting Point M-565 Operation Manual, Version DTable 3-2: Optional accessories (cont.)Product Order numberCompact keyboard German

3 Technical data13 Melting Point M-565 Operation Manual, Version DTable 3-2: Optional accessories (cont.)Product Order numberIQ/OQ: After installatio

3 Technical data14 Melting Point M-565 Operation Manual, Version D3.2 Technical data overviewTable 3-3: Technical data of the Melting Point M-565Mel

3 Technical data15 Melting Point M-565 Operation Manual, Version DTable 3-3: Technical data of the Melting Point M-565 (cont.)Melting Point M-565Stor

4 Description of function16 Melting Point M-565 Operation Manual, Version D4 Description of functionThis section explains the basic principle of the

4 Description of function17 Melting Point M-565 Operation Manual, Version D4.1.1 Pharmacopoeia and thermodynamic melting pointsThe melting process o

4 Description of function18 Melting Point M-565 Operation Manual, Version D4.1.2 Boiling pointsThe boiling point is determined by the “Siwoloboff” m

4 Description of function19 Melting Point M-565 Operation Manual, Version D4.2 Controls and connectionsabcdefa Power switch; turns the instrument on

5 Putting into operation20 Melting Point M-565 Operation Manual, Version D5 Putting into operationThis section describes the installation of the Mel

5 Putting into operation21 Melting Point M-565 Operation Manual, Version D• Glass window • Glass window with glass holder• Install the glass wind

5 Putting into operation22 Melting Point M-565 Operation Manual, Version DAccessories• Place the melting point capillaries in the hole of the housi

6 Operation23 Melting Point M-565 Operation Manual, Version D6 OperationThis section explains the operating elements and possible operating modes. It

6 Operation24 Melting Point M-565 Operation Manual, Version DDifferent menus can be accessed by turning the rotary knob. Each menu has its own symbol.

6 Operation25 Melting Point M-565 Operation Manual, Version DScreen during melting point determinationSettings menuResult indication (numeric result)

6 Operation26 Melting Point M-565 Operation Manual, Version D6.1.4 Using the external keyboardNOTEThe instrument can be operated using an external ke

6 Operation27 Melting Point M-565 Operation Manual, Version DPreparation of the samples:• The samples being investigated must be fully dry, homogeno

6 Operation28 Melting Point M-565 Operation Manual, Version DNOTEInsert samples only when the start temperature is reached (as soon as prompted).• P

6 Operation29 Melting Point M-565 Operation Manual, Version D• To run through the results, turn the rotary knob up and down.• To replay the record

Table of contents3 Melting Point M-565 Operation Manual, Version DTable of contents1 About this manual . . . . . . . . . . . . . . . . . . . . . . .

6 Operation30 Melting Point M-565 Operation Manual, Version D6.2.3 Creating a methodInstead of entering and using the parameters directly from the id

6 Operation31 Melting Point M-565 Operation Manual, Version D• Turn the rotary knob to select a method.• Press START to start the determination.•

6 Operation32 Melting Point M-565 Operation Manual, Version D6.2.7 Melting resultNOTEChanging the determination mode does not affect the principle of

6 Operation33 Melting Point M-565 Operation Manual, Version DabcdefghiPrintouta Instrument typeb Determination parametersc Automatically detected resu

6 Operation34 Melting Point M-565 Operation Manual, Version D6.2.7.2 Melting range• In the settings, change the melting result to Melting range and

6 Operation35 Melting Point M-565 Operation Manual, Version DabcdefghiPrintouta Instrument typeb Determination parametersc Automatically detected resu

6 Operation36 Melting Point M-565 Operation Manual, Version D6.2.7.3 Melting point thermodynamic• In the settings, change the melting result to Mel

6 Operation37 Melting Point M-565 Operation Manual, Version DabcdefghidPrintouta Instrument typeb Determination parametersc Correction factor for the

6 Operation38 Melting Point M-565 Operation Manual, Version D6.3 Boiling pointNOTEFor exact boiling point determination, use boiling point tubes and

6 Operation39 Melting Point M-565 Operation Manual, Version D• Use the rotary knob to choose the start tempera-ture and press Next.• Use the rotar

Table of contents4 Melting Point M-565 Operation Manual, Version D6 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 Operation40 Melting Point M-565 Operation Manual, Version D73.2 76.473.4 76.6Delay: to ensure equilibrium between oven temperature and sample temper

6 Operation41 Melting Point M-565 Operation Manual, Version DWhen a measurement is done, the last method parameters are always retained in the instrum

6 Operation42 Melting Point M-565 Operation Manual, Version D6.4 CalibrationNOTEBUCHI recommends calibrating each new instrument after installation.

6 Operation43 Melting Point M-565 Operation Manual, Version D6.4.2 Calibration procedureTo start calibration, turn the rotary knob to Calibration. Pr

6 Operation44 Melting Point M-565 Operation Manual, Version D6.4.3 PrintoutabcdegfhPrintouta Instrument typeb General information regarding calibra

6 Operation45 Melting Point M-565 Operation Manual, Version D6.4.4 VerificationTo verify the calibration, proceed as follows:• Measure all standards

6 Operation46 Melting Point M-565 Operation Manual, Version D• Press the Test button to enter the functional test, and follow the instructions.•

6 Operation47 Melting Point M-565 Operation Manual, Version DTable 6-1: Setting parameters (cont.)Thermodynamic correction 0.0–3.0; default value: 1.1

6 Operation48 Melting Point M-565 Operation Manual, Version D6.5.1 Test protocolabca Power supply voltageb Values for sample brightnessc Signature o

6 Operation49 Melting Point M-565 Operation Manual, Version D6.5.2 SysInfo protocolaa Setting parameters

1 About this manual5 Melting Point M-565 Operation Manual, Version D1 About this manualThis manual describes the Melting Point M-565 and provides al

7 Maintenance50 Melting Point M-565 Operation Manual, Version D7 MaintenanceThis section provides instructions on all maintenance work to be performe

7 Maintenance51 Melting Point M-565 Operation Manual, Version D7.4 Cleaning the heating blockRemove broken capillaries from the heating block.ATTENTI

8 Troubleshooting52 Melting Point M-565 Operation Manual, Version D8 TroubleshootingThe following section describes how to resume operation of the in

8 Troubleshooting53 Melting Point M-565 Operation Manual, Version DTable 8-1: General malfunctions and their remedyMalfunction Possible cause RemedySa

8 Troubleshooting54 Melting Point M-565 Operation Manual, Version DTable 8–4: Error messagesError number Possible cause RemedyError 11 Internal clock,

9 Shutdown, storage, transport and disposal55 Melting Point M-565 Operation Manual, Version D9 Shutdown, storage, transport, and disposalThis sectio

10 Spare parts56 Melting Point M-565 Operation Manual, Version D10 Spare partsThis section lists spare parts, accessories, and optional extras, incl

11 Declarations and requirements57 Melting Point M-565 Operation Manual, Version D11 Declarations and requirements11.1 FCC requirements (for USA an

11 Declarations and requirements58 Melting Point M-565 Operation Manual, Version D11.2 Declaration of conformity

2 Safety6 Melting Point M-565 Operation Manual, Version D2 SafetyThis section highlights the safety concept of the Melting Point M-565, Sample Loader

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2 Safety7 Melting Point M-565 Operation Manual, Version D2.4 Warning notices used in this manualWARNINGGenerally, the triangular warning symbol indic

2 Safety8 Melting Point M-565 Operation Manual, Version D2.5.3 Safety measuresAlways wear personal protective equipment such as protective goggles an

3 Technical data9 Melting Point M-565 Operation Manual, Version D3 Technical dataThis section introduces the reader to the Melting Point M-565 and i