Buchi Syncor Polyvap Bedienungsanleitung

Operation Manual093013 enAccessoriesSyncore®

Syncore® Accessories8 version EFigure 13: Inert gas cover complete1 Scope of deliveryInert gas cover R-2441918Consisting of:1 Vacuum cover, no glas

Syncore® Accessoriesversion E 92 Safety2 SafetyThis unit and all its components have been built in ac-cordance with the state of the art and re

Syncore® Accessories10 version ESyncore Polyvap/Syncore single platformwith accessories:• Parallelevaporationofsolventsinvariousformatsand

Syncore® Accessoriesversion E 112.5 Basic hazards The basic hazards arise from:• Chemicalsthataretoxicorcauseallergicreactions,orcan, in a

Syncore® Accessories12 version E2.7 ModificationsNo modifications may be made on this unit or on spare and accessory parts, nor is use of spar

Syncore® Accessoriesversion E 133.1 Syncore Product Line AccessoriesThe Syncore product line is modular throughout. Every ac-cessory is usable at any

Syncore® Accessories14 version EFunction,putting into operation, operation and maintenace• Fastenthecoldwatersupplytotheconnectionunits a

Syncore® Accessoriesversion E 153.3 RacksIntroductionThe Syncore product line allows various racks to be used on a given platform. These permit the p

Syncore® Accessories16 version ESample volume (SV)Rack Minimum SV Optimum SVR-4 50 ml 500 mlR-4 with residual vol. 50 ml 500 mlR-6 25 ml 250 mlR-6

Syncore® Accessoriesversion E 17Use only clean distilled water.Whenever the racks are not going to be used for a prolon-ged time, empty them so as to

Syncore® Accessories18 version EEmpty positionsDue to active cooling of the residual volume appendages on the glasses in the Rack R-6 with cooling

Syncore® Accessoriesversion E 19Rack R-12Rack R-12 provides for the heating or cooling of test vessels with rounded bases. Only those glass vessels d

Syncore® Accessories20 version ECustomer-specific racksIt is possible to build a customer-specific rack with various glass geometries and sizes. Unde

Syncore® Accessoriesversion E 213.4 Vacuum coversIntroductionThe vacuum connection is used in conjunction with a sui-table vacuum source in order to

Syncore® Accessories22 version EFigure 24: 24 V connection on the vacuum connectionElectrical connectionConnect the plug a on the electrical cable

Syncore® Accessoriesversion E 23To ensure a quick warming of the vacuum connection, the vortex drive should not be switched ON. A flashing in the disp

Syncore® Accessories24 version EGlass plateThe glass plate lets the operator observe the vacuum zone inside the vacuum connection. The operator can

Syncore® Accessoriesversion E 25Maintenance of the vacuum connectionThe gas plates of the vacuum connections can be removed by releasing the two clam

Syncore® Accessories26 version E3.5 Cooling plateIntroductionThe cooling plate b is installed between the base plate a of the unit and a rack c. Wh

Syncore® Accessoriesversion E 27Then screw the holding clamps onto the cooling plate. A Rack can now be put on, just as on the base plate.It is impor

Syncore® Accessoriesversion E 11 Scope of delivery 21.1 Racks 21.2 Glass tubes and holders 31.3 Vacuum covers 51.4 Condenser units 51.5 In

Syncore® Accessories28 version E3.6 ValvesFor all types of valves: Always secure the connections! Poorly secured hose connections can resullt

Syncore® Accessoriesversion E 293.7 Inert gas cover / inert gas moduleUsing the inert gas cover, 24 reaction glass vessels can be simultaneously sea

Syncore® Accessories30 version EFunction testTightnessTightness is tested at slight gas excess pressure.To do so, the vacuum connection must be sea

Syncore® Accessoriesversion E 31Figure 39: Hose coupling diagramFor sensitive reactions where traces of steam or other ga-ses can cause disturbances,

Syncore® Accessories32 version EDirect concentrationWe recommend direct concentration of reaction mixtures for sensitive reaction products, which a

Syncore® Accessoriesversion E 33Maintenance of the intert gas moduleYou can use organic solvents like ethanol or acetone to remove organic residues.

Syncore® Accessories34 version E3.8 Reflux module/flushback moduleThe reflux module/flushback module a enables simulta-neous condensation of solvent va

Syncore® Accessoriesversion E 35Setting upAmong others, the reflux module/flushback module con-sists of two metal plates with recesses for the individu

Syncore® Accessories36 version ETemperature of the cooling mediumThe ideal choice of the coolant temperature is depending on the boling point of th

Syncore® Accessoriesversion E 37Removing the reflux/flushback moduleYou can only remove the reflux/flushback module from the rack, after you have turned

Syncore® Accessories2 version E1.1 RacksCrystal Rack R-4 Order Code1 Rack R-4 for working volume of up to 4 x 500ml, incl. 4 glasses R-4 4

Syncore® Accessories38 version EFigure 47: Replacement parts, Rack R-244 Replacement parts 4076441829Only original accessory and spare parts ensure

Syncore® Accessoriesversion E 39Figure 50: Holder for vessel R-4Rack R-48 and R-961 Set of 100 balancing springs407651 Threaded Rack bar409344.2 Glas

Syncore® Accessories40 version EHolder for R-6 vessels (Analyst or Polyvap)1 Holder for 6 Syncore Analyst or Polyvap vessels 38483Vessels R-12

Syncore® Accessoriesversion E 41Figure 53: Replacement parts, vacuum cover R-4Figure 54: Replacement parts, vacuum cover R-4Figure 55: Replacement pa

Syncore® Accessories42 version EFigure 57: Replacement parts, vacuum cover R-12Figure 58: Replacement parts, vacuum cover R-12Figure 59: Replacemen

Syncore® Accessoriesversion E 43Figure 61: Replacement parts, vacuum cover R-96Figure 62: Replacement parts, vacuum cover R-9638490418383849538178384

Syncore® Accessories44 version EFigure 63: Condenser unit S4.4 Condenser units376930327527344376863769440653Condenser unit S complete(PLASTIC + GLA

Syncore® Accessoriesversion E 45Figure 64: Condenser unit CCondenser unit C complete(PLASTIC + GLAS) Order code1 Condenser unit C complete, 1 Li

Syncore® Accessories46 version E Order code1 Set of 50 butyl septa, with PTFE coating494891Setaus6PEEKSepten- Verschraubungen419191 Set

Syncore® Accessoriesversion E 4741925384964294331356Components Order code1 Vacuum hose to vacuum cover length: 1m 260961 Water hose, length: 1

Syncore® Accessoriesversion E 31.2 Glass tubes and holders Order codeVessels R-4 without resi

Syncore® Accessories48 version E5 Appendix5.1 Technical dataConnection to inert gas module cpl.,vacuum connection24 VPower take-up for the vacuum c

Syncore® Accessoriesversion E 495.3 Table of solventsStarting pressure to reduce the boiling point to 40 °CSolvent Formula Molecular weightin g/molEn

Syncore® Accessories50 version EResistance of polyethylene sealing discsA: Very good resistance: Sealing discs of PE (polyethylene) may be used wi

Syncore® Accessoriesversion E 51Resistance of FPM A: Very good resistance: FPM may be used without rest-rictions B: Moderate resistance: Sealing

Syncore® Accessories52 version ESolvent ResistanceAcetaldehyde BAcetone ABenzene DButanol BChloroform DDiethyl ether CDimethylformamide ADime

Syncore® Accessoriesversion E 53Solvent ResistanceAcetaldehyde BAcetone ABenzene AButanol AChloroform ADiethyl ether ADimethylformamide ADimeth

Syncore® Accessories54 version ESolvent ResistanceAcetaldehyde AAcetone ABenzene AButanol AChloroform ADiethyl ether ADimethylformamide ADime

Syncore® Accessoriesversion E 55English:This equipment has been tested and found to comply with the limits for a Class A digital device, pusuant to b

Syncore® Accessories56 version E5.5 Declaration of Conformity5 Appendix

Syncore® Accessories4 version EVessels R-12 without residual volume (Polyvap)(Ø: 48 mm / H: 147 mm / Vol.: 120 ml)1 Set of 12 vessels for Rack R-12

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Syncore® Accessoriesversion E 5Figure 6: Condenser unit SFigure 7: Condenser unit CFigure 5: Vacuum covers1 Scope of delivery1.3 Vacuum covers Vacuum

Syncore® Accessories6 version E1.5 Insulation for high boiling solvents Insulation for high boiler to Rack R-2441922Consisting of:1 Insulation plat

Syncore® Accessoriesversion E 71.7 Low temperature insulationInsulation to Rack R-24 and Rack R-96, cpl.1 Insulation complete to Rack R-24 and Ra