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Buchi DuMaster D-480 Handbücher

Bedienungsanleitungen und Benutzerhandbücher für Messgeräte Buchi DuMaster D-480.
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Buchi DuMaster D-480 Bedienungsanleitung (356 Seiten)


Marke: Buchi | Kategorie: Messgeräte | Größe: 3.22 MB |

 

Inhaltsverzeichnis

DuMaster D-480

1

Operation Manual

1

Copyright Note 3

3

Contents

5

Contents 6

6

Contents 7

7

Contents 8

8

Contents 9

9

Contents 10

10

Contents 11

11

General

13

Revision history

14

About this document

15

Display conventions

16

Basic security settings

17

Warning: residual risks

19

Gas supply

20

Temperature monitoring

20

Instrument casing

20

Protective earth conductor

21

Waste gas lines

21

Warning sign furnace

22

Warning sign electrical area

22

Meaning of the warning signs

22

Safe instrument

23

Warning

23

Knowledge and skills

23

Protective glasses

24

Protective gloves

24

Laboratory clothing

24

Damaged base panel

25

Gas pressure

25

Hot instrument parts

25

Changing mode

25

Removing reaction tubes

26

Filling reaction tubes

26

Filling the drying tube

27

Product description

29

3 - Product description 30

30

Analytical characteristics

31

Technical specifications

31

Dimensions and weights

32

Electrical and gas supply

32

Ambient conditions

32

Instrument design

33

Front view

34

Furnace section

35

Rear view

36

Right side view

37

Left side view

38

Top view

39

CHAPTER 4

41

Functional units

43

Symbols

44

dosing system (I)

44

Introduction

48

Setting device parameters

50

Instrument equipment

51

Calibration formulae

55

Routine measuring work

56

Instrument blank values

57

Conditioning samples

57

Daily factor determinations

57

Blank value determination

58

Blank value compensation

58

Daily factor

58

Software user interface

61

Sample view

62

Sample view input functions

63

Color coding

63

Combi view

64

Statistics view

66

Calibration view

66

Status view

67

Right mouse button function

69

In dialogs

70

Further functions

70

Copyright Note 71

71

Copyright Note 72

72

21 CFR Part 11 functionality

73

Versioning

74

Work performed by the system

75

Conditions for installation

76

Requirements for operation

76

Configure analyzer

77

Defining logon timeout

78

Creating new sections

79

LIMS export settings

81

User administration

83

Granting authorizations

83

Defining interfaces

85

Dialog details

87

Editing analysis data

88

Performing checks

90

Viewing the logbook

92

Working with the database

93

Database

94

Database backup

95

Starting the database backup

96

Reorganize database

96

Analyzer configuration

99

Reacting to irregularities

99

Sleep/wake-up behavior

99

Optimizing data evaluation

101

Modifying the registration

103

Printer setup

103

CHAPTER 6

105

First-time start-up

107

General requirements

107

Specific requirements

108

Start-up

109

Connecting peripherals

110

Peripherals

111

Configuring the balance

111

Switching on

114

Default instrument settings

114

intake pressure

115

Flow rate

115

Shutting down the instrument

116

Procedure

117

Safety instruction

118

Using the instrument

119

Measurement settings

120

Keywords

121

Factory-set key words

121

Defining custom keywords

121

Viewing the list

121

Configuring error handling

124

Preparing samples

125

Determining sample weight

126

Packing samples

127

Preparing measurement work

129

Software usage rules

130

Waking up the instrument

130

Selecting the operating mode

131

Viewing method settings

131

Defining custom methods

131

Defining the Kjeldahl factor

132

Copy methods

133

Settings for sample input

133

Importing weighing data

134

Prioritizing urgent samples

134

What can you optimize?

135

Performing measurement work

136

Values for oxygen dosing

137

Performing measurements

138

Overview

140

Purpose

142

Checklist

142

Background

143

Determining blank values

144

Determining the daily factor

145

Stopping continuous analysis

147

Configuring the sample view

149

Saving the sample view

150

Loading a sample view

150

Configure statistics view

150

Generating statistical data

150

Statistical data

151

Manual peak integration

152

Single peaks

153

Superimposed peaks

153

Melted peaks

153

Manual integratability

154

Baseline

154

Integration of single peaks

154

Configuring the graph view

156

Configure report

157

Display print preview

157

Data backup and printing

158

Export and import

159

Exporting LIMS data

160

Working with documents

161

Creating new documents

162

Editing documents

162

Deleting documents

163

Finding documents

163

Finding previous versions

164

What can you copy?

164

Selecting cells

164

Inserting data

164

Importing documents

165

Signing documents

165

What signature is checked?

166

Checking a signature

166

Maintaining the instrument

167

Recommendation

169

Installing used tubes

171

Safety instruction

172

Purpose of conditioning

172

Types of conditioning

172

Flushing tubes

173

Performing the calibration

175

Defining standard substances

176

Process

178

Requirements:

178

Displayed characteristics

182

Quality factor "r"

183

Coefficient "a"

183

Calibration tables

185

Suggestion

186

Replacing the ash crucible

187

Removing the ash crucible

188

Furnace area

189

Top view furnace

189

Installing the ash crucible

191

Replacing sealing elements

193

Removing sealing elements

195

Ball valve maintenance

196

Dismantled ball valve

199

Requirements

202

Installing the Ni flap

209

Installing the O

212

Purpose of cleaning

218

Cleaning the carousel

218

Emptying reaction tubes

221

Filling the combustion tube

222

Filling the reduction tube

224

In this section

226

Filling the drying tubes

234

Drying tube filling (large)

235

Repairing the instrument

239

Software reaction to errors

240

On-screen error message

240

Interpreting error code

240

Performing a system test

241

Performing a leak test

242

Leak test procedure

243

Replacing fuses

243

Fuse holder

244

Phase 3: Insert fuses

246

After a computer crash

247

Reacting to a power failure

248

When is this necessary?

251

Changing the position

251

Export for support

251

Exporting analysis data

252

Menu and dialog descriptions

253

Dialog descriptions key

254

File menu

255

File > New (Command)

256

Listbox columns

257

Select version (Dialog)

258

Save file as (Dialog)

259

File > Delete (Command)

260

Sign (Dialog)

261

Export to LIMS (Dialog)

262

Configure report (Dialog)

263

Elements

264

Further information

264

Print (Dialog)

265

Print preview (Dialog)

266

Printer setup (Dialog)

267

Open (Dialog)

268

Load balance file (Dialog)

269

Configure backup (Dialog)

269

Clean database (Dialog)

271

Restore database (Dialog)

271

Log in as (Dialog)

272

File > Logoff (Command)

273

File > Exit (Command)

273

Edit menu

274

Edit > Redo (Command)

275

Edit > Undo (Command)

275

Edit > Cut (Command)

275

Edit > Copy (Command)

275

Edit > Paste (Command)

276

Swap samples (Dialog)

277

Edit > Modify (Command)

277

Set stop tag (Dialog)

278

View menu

281

View > Toggle (Command)

282

Zoom in/out (Dialog)

282

Configure view (Dialog)

282

Column properties (Dialog)

283

Save views (Dialog)

284

Load views (Dialog)

285

Delete views (Dialog)

285

Function

286

Select columns (Dialog)

288

System menu

289

System > Stop (Command)

290

Feeding (Dialog)

291

Analysis mode (Dialog)

293

Windows menu

295

Toolbar

296

Weighing window (Dialog)

297

Options menu

299

Replace part (Dialog)

301

Leak test (Dialog)

302

System test (Dialog)

304

Error buffer (Dialog)

306

Error display (Dialog)

306

Input options (Dialog)

307

Standard samples (Dialog)

308

Keywords (Dialog)

309

Acoustic signals (Dialog)

310

LIMS settings (Dialog)

311

"LIMS data" tab

312

"Identifier" tab:

313

Device parameters (Dialog)

314

Method (Dialog)

315

Error handling (Dialog)

316

Monthly logbook (Dialog)

319

Select period (Dialog)

320

"DEVICE.INI" tab

321

Configure key value (Dialog)

323

Math menu

325

Blank values (Dialog)

326

Math. > Factor (Command)

327

Define type of peak (Dialog)

327

Area assignment (Dialog)

328

Statistics menu

331

Calibration menu

334

Help menu

339

Help > Content (Command)

340

Help > Find (Command)

340

Short cuts

341

Appendix

343

Warranty

344

Warranty on the furnace

345

11 - Appendix 346

346

Smallest workable unit

347

Required accessories

347

Optional accessories

348

11 - Appendix 349

349

Index 351

351

Index 352

352

Index 353

353

Index 354

354

Quality in your hands

356

Find your BUCHI Contacts:

356
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